HEADER HYDROLASE (SERINE PROTEINASE) 26-OCT-81 3PTN 3PTN 3 COMPND TRYPSIN (TRIGONAL, 2.4 M AMMONIUM SULFATE) (E.C.3.4.21.4) 3PTN 4 SOURCE BOVINE (BOS TAURUS) PANCREAS 3PTN 5 AUTHOR J.WALTER,W.STEIGEMANN,T.P.SINGH,H.BARTUNIK,W.BODE,R.HUBER 3PTN 6 REVDAT 6 09-APR-85 3PTNE 1 JRNL 3PTNE 1 REVDAT 5 14-MAR-85 3PTND 3 SEQRES ATOM 3PTND 1 REVDAT 4 23-FEB-84 3PTNC 1 REMARK 3PTNC 1 REVDAT 3 30-SEP-83 3PTNB 1 REVDAT 3PTNB 1 REVDAT 2 15-APR-82 3PTNA 1 REMARK 3PTNB 2 REVDAT 1 04-MAR-82 3PTN 0 3PTNB 3 JRNL AUTH J.WALTER,W.STEIGEMANN,T.P.SINGH,H.BARTUNIK,W.BODE, 3PTN 7 JRNL AUTH 2 R.HUBER 3PTN 8 JRNL TITL ON THE DISORDERED ACTIVATION DOMAIN IN 3PTN 9 JRNL TITL 2 TRYPSINOGEN. CHEMICAL LABELLING AND 3PTNE 2 JRNL TITL 3 LOW-*TEMPERATURE CRYSTALLOGRAPHY 3PTNE 3 JRNL REF ACTA CRYSTALLOGR.,SECT.B V. 38 1462 1982 3PTNE 4 JRNL REFN ASTM ACBCAR DK ISSN 0567-7408 107 3PTNE 5 REMARK 1 3PTN 14 REMARK 1 REFERENCE 1 3PTNC 2 REMARK 1 AUTH M.MARQUART,J.WALTER,J.DEISENHOFER,W.BODE,R.HUBER 3PTNC 3 REMARK 1 TITL THE GEOMETRY OF THE REACTIVE SITE AND OF THE 3PTNC 4 REMARK 1 TITL 2 PEPTIDE GROUPS IN TRYPSIN, TRYPSINOGEN AND ITS 3PTNC 5 REMARK 1 TITL 3 COMPLEXES WITH INHIBITORS 3PTNC 6 REMARK 1 REF ACTA CRYSTALLOGR.,SECT.B V. 39 480 1983 3PTNC 7 REMARK 1 REFN ASTM ASBSDK DK ISSN 0108-7681 622 3PTNC 8 REMARK 1 REFERENCE 2 3PTNC 9 REMARK 1 AUTH H.FEHLHAMMER,W.BODE,R.HUBER 3PTN 16 REMARK 1 TITL CRYSTAL STRUCTURE OF BOVINE TRYPSINOGEN AT 1.8 3PTN 17 REMARK 1 TITL 2 ANGSTROMS RESOLUTION. /II$. CRYSTALLOGRAPHIC 3PTN 18 REMARK 1 TITL 3 REFINEMENT, REFINED CRYSTAL STRUCTURE AND 3PTN 19 REMARK 1 TITL 4 COMPARISON WITH BOVINE TRYPSIN 3PTN 20 REMARK 1 REF J.MOL.BIOL. V. 111 415 1977 3PTN 21 REMARK 1 REFN ASTM JMOBAK UK ISSN 0022-2836 070 3PTNA 1 REMARK 1 REFERENCE 3 3PTNC 10 REMARK 1 AUTH W.BODE,P.SCHWAGER,R.HUBER 3PTN 24 REMARK 1 TITL STRUCTURAL STUDIES ON THE PANCREATIC TRYPSIN 3PTN 25 REMARK 1 TITL 2 INHIBITOR-TRYPSIN COMPLEX AND ITS FREE COMPONENTS. 3PTN 26 REMARK 1 TITL 3 STRUCTURE AND FUNCTION RELATIONSHIPS IN SERINE 3PTN 27 REMARK 1 TITL 4 PROTEASE INHIBITION AND CATALYSIS 3PTN 28 REMARK 1 REF MIAMI WINTER SYMP. V. 11 43 1976 3PTN 29 REMARK 1 REFN ASTM MIWSAE US ISSN 0097-0808 926 3PTN 30 REMARK 1 REFERENCE 4 3PTNC 11 REMARK 1 AUTH W.BODE,P.SCHWAGER 3PTN 32 REMARK 1 TITL THE REFINED CRYSTAL STRUCTURE OF BOVINE 3PTN 33 REMARK 1 TITL 2 BETA-*TRYPSIN AT 1.8 ANGSTROMS RESOLUTION. 3PTN 34 REMARK 1 TITL 3 /II$. CRYSTALLOGRAPHIC REFINEMENT, CALCIUM BINDING 3PTN 35 REMARK 1 TITL 4 SITE, BENZAMIDINE BINDING SITE AND ACTIVE SITE AT 3PTN 36 REMARK 1 TITL 5 $P*H 7.0 3PTN 37 REMARK 1 REF J.MOL.BIOL. V. 98 693 1975 3PTN 38 REMARK 1 REFN ASTM JMOBAK UK ISSN 0022-2836 070 3PTN 39 REMARK 1 REFERENCE 5 3PTNC 12 REMARK 1 AUTH H.FEHLHAMMER,W.BODE 3PTN 41 REMARK 1 TITL THE REFINED CRYSTAL STRUCTURE OF BOVINE 3PTN 42 REMARK 1 TITL 2 BETA-*TRYPSIN AT 1.8 ANGSTROMS RESOLUTION. 3PTN 43 REMARK 1 TITL 3 I. CRYSTALLIZATION, DATA COLLECTION AND APPLICATION 3PTN 44REMARK 1 TITL 4 OF PATTERSON SEARCH TECHNIQUES 3PTN 45 REMARK 1 REF J.MOL.BIOL. V. 98 683 1975 3PTN 46 REMARK 1 REFN ASTM JMOBAK UK ISSN 0022-2836 070 3PTN 47 REMARK 1 REFERENCE 6 3PTNC 13 REMARK 1 AUTH W.BODE,P.SCHWAGER 3PTN 49 REMARK 1 TITL THE SINGLE CALCIUM-BINDING SITE OF CRYSTALLINE 3PTN 50 REMARK 1 TITL 2 BOVINE BETA-TRYPSIN 3PTN 51 REMARK 1 REF /FEBS$ LETT. V. 56 139 1975 3PTN 52 REMARK 1 REFN ASTM FEBLAL NE ISSN 0014-5793 165 3PTN 53 REMARK 1 REFERENCE 7 3PTNC 14 REMARK 1 EDIT M.O.DAYHOFF 3PTN 55 REMARK 1 REF ATLAS OF PROTEIN SEQUENCE V. 5 105 1972 3PTN 56 REMARK 1 REF 2 AND STRUCTURE (DATA SECTION) 3PTN 57 REMARK 1 PUBL NATIONAL BIOMEDICAL RESEARCH FOUNDATION, 3PTN 58 REMARK 1 PUBL 2 SILVER SPRING,MD. 3PTN 59 REMARK 1 REFN ISBN 0-912466-02-2 435 3PTN 60 REMARK 2 3PTN 61 REMARK 2 RESOLUTION. 1.7 ANGSTROMS. 3PTN 62 REMARK 3 3PTN 63 REMARK 3 REFINEMENT. DEISENHOFER*S VERSION OF THE JACK AND LEVITT 3PTN 64 REMARK 3 REFINEMENT PROCEDURE COMBINING CRYSTALLOGRAPHIC AND ENERGY 3PTN 65 REMARK 3 REFINEMENT. THE DIAGONAL-MATRIX LEAST-SQUARES METHOD WAS 3PTN 66 REMARK 3 ALSO USED TO REFINE ISOTROPIC TEMPERATURE FACTORS. 3PTN 67 REMARK 3 (A.JACK,M.LEVITT,ACTA CRYST.,A34,931-935,1978). 3PTN 68 REMARK 3 THE R-VALUE FOR REFLECTIONS WITHIN THE SHELL 1.7 TO 6.5 3PTN 69 REMARK 3 ANGSTROMS IS 0.198. 3PTN 70 REMARK 4 3PTN 71 REMARK 4 AN OCCUPANCY OF 0.0 INDICATES THAT NO SIGNIFICANT ELECTRON 3PTN 72 REMARK 4 DENSITY WAS FOUND IN THE FINAL FOURIER MAP. 3PTN 73 REMARK 5 3PTNA 2 REMARK 5 CORRECTION. INSERT MISSING CODEN FOR REFERENCE 1. 3PTNA 3 REMARK 5 15-APR-82. 3PTNA 4 REMARK 6 3PTNB 4 REMARK 6 CORRECTION. INSERT REVDAT RECORDS. 30-SEP-83. 3PTNB 5 REMARK 7 3PTNC 15 REMARK 7 CORRECTION. INSERT NEW PUBLICATION AS REFERENCE 1 AND 3PTNC 16 REMARK 7 RENUMBER THE OTHERS. 23-FEB-84. 3PTNC 17 REMARK 8 3PTND 2 REMARK 8 CORRECTION. CHANGE RESIDUE 165 FROM ASN TO ASP AND CHANGE 3PTND 3 REMARK 8 RESIDUE 186 FROM GLN TO GLU, UPON DEPOSITORS INSTRUCTIONS. 3PTND 4 REMARK 8 REVISE ATOM AND SEQRES RECORDS ACCORDINGLY. 14-MAR-85. 3PTND 5 REMARK 9 3PTNE 6 REMARK 9 CORRECTION. UPDATE JRNL REFERENCE TO REFLECT PUBLICATION. 3PTNE 7 REMARK 9 09-APR-85. 3PTNE 8 SEQRES 1 223 ILE VAL GLY GLY TYR THR CYS GLY ALA ASN THR VAL PRO 3PTN 74 SEQRES 2 223 TYR GLN VAL SER LEU ASN SER GLY TYR HIS PHE CYS GLY 3PTN 75 SEQRES 3 223 GLY SER LEU ILE ASN SER GLN TRP VAL VAL SER ALA ALA 3PTN 76 SEQRES 4 223 HIS CYS TYR LYS SER GLY ILE GLN VAL ARG LEU GLY GLU 3PTN 77 SEQRES 5 223 ASP ASN ILE ASN VAL VAL GLU GLY ASN GLU GLN PHE ILE 3PTN 78 SEQRES 6 223 SER ALA SER LYS SER ILE VAL HIS PRO SER TYR ASN SER 3PTN 79 SEQRES 7 223 ASN THR LEU ASN ASN ASP ILE MET LEU ILE LYS LEU LYS 3PTN 80 SEQRES 8 223 SER ALA ALA SER LEU ASN SER ARG VAL ALA SER ILE SER 3PTN 81 SEQRES 9 223 LEU PRO THR SER CYS ALA SER ALA GLY THR GLN CYS LEU 3PTN 82 SEQRES 10 223 ILE SER GLY TRP GLY ASN THR LYS SER SER GLY THR SER 3PTN 83 SEQRES 11 223 TYR PRO ASP VAL LEU LYS CYS LEU LYS ALA PRO ILE LEU 3PTN 84 SEQRES 12 223 SER ASP SER SER CYS LYS SER ALA TYR PRO GLY GLN ILE 3PTND 6 SEQRES 13 223 THR SER ASN MET PHE CYS ALA GLY TYR LEU GLU GLY GLY 3PTND 7 SEQRES 14 223 LYS ASP SER CYS GLN GLY ASP SER GLY GLY PRO VAL VAL 3PTN 87 SEQRES 15 223 CYS SER GLY LYS LEU GLN GLY ILE VAL SER TRP GLY SER 3PTN 88 SEQRES 16 223 GLY CYS ALA GLN LYS ASN LYS PRO GLY VAL TYR THR LYS 3PTN 89 SEQRES 17 223 VAL CYS ASN TYR VAL SER TRP ILE LYS GLN THR ILE ALA 3PTN 90 SEQRES 18 223 SER ASN 3PTN 91 FTNOTE 1 3PTN 92 FTNOTE 1 SEE REMARK 4. 3PTN 93 HET CA 480 1 CALCIUM (II) ION 3PTN 94 FORMUL 2 CA CA1 ++ 3PTN 95 FORMUL 3 HOH *82(H2 O1) 3PTN 96 HELIX 1 H1 SER 164 ILE 176 1 SNGL ALPHA TURN,REST IRREG. 3PTN 97 HELIX 2 H2 LYS 230 VAL 235 5 CONTIGUOUS WITH H3 3PTN 98 HELIX 3 H3 SER 236 ASN 245 1 CONTIGUOUS WITH H2 3PTN 99 SSBOND 1 CYS 22 CYS 157 3PTN 100 SSBOND 2 CYS 42 CYS 58 3PTN 101 SSBOND 3 CYS 128 CYS 232 3PTN 102 SSBOND 4 CYS 136 CYS 201 3PTN 103 SSBOND 5 CYS 168 CYS 182 3PTN 104 SSBOND 6 CYS 191 CYS 220 3PTN 105 CRYST1 55.110 55.110 109.380 90.00 90.00 120.00 P 31 2 1 6 3PTN 106 ORIGX1 1.000000 .577350 0.000000 0.00000 3PTN 107 ORIGX2 0.000000 1.154701 0.000000 0.00000 3PTN 108 ORIGX3 0.000000 0.000000 1.000000 0.00000 3PTN 109 SCALE1 .018146 .010476 0.000000 0.00000 3PTN 110 SCALE2 0.000000 .020953 0.000000 0.00000 3PTN 111 SCALE3 0.000000 0.000000 .009142 0.00000 3PTN 112 ATOM 1 N ILE 16 51.997 15.638 48.154 1.00 16.35 3PTN 113 ATOM 2 CA ILE 16 52.054 14.531 49.128 1.00 16.35 3PTN 114 ATOM 3 C ILE 16 53.326 14.579 49.971 1.00 16.35 3PTN 115 ATOM 4 O ILE 16 54.442 14.581 49.399 1.00 16.35 3PTN 116 ATOM 5 CB ILE 16 52.014 13.177 48.379 1.00 16.35 3PTN 117 ATOM 6 CG1 ILE 16 50.788 13.051 47.452 1.00 17.77 3PTN 118 ATOM 7 CG2 ILE 16 52.126 11.959 49.318 1.00 17.77 3PTN 119 ATOM 8 CD1 ILE 16 49.487 12.807 48.245 1.00 17.77 3PTN 120 ATOM 9 N VAL 17 53.168 14.567 51.274 1.00 13.81 3PTN 121 ATOM 10 CA VAL 17 54.289 14.479 52.218 1.00 13.81 3PTN 122 LOCUS BTTRYPAP 805 bp RNA MAM 06-JUN-1991 DEFINITION Bovine mRNA for pancreatic anionic trypsinogen. ACCESSION X54703 KEYWORDS trypsin. SOURCE cow. ORGANISM Bos taurus Eukaryotae; mitochondrial eukaryotes; Metazoa/Eumycota group; Metazoa; Eumetazoa; Bilateria; Coelomata; Deuterostomia; Chordata; Vertebrata; Gnathostomata; Osteichthyes; Sarcopterygii; Choanata; Tetrapoda; Amniota; Mammalia; Theria; Eutheria; Artiodactyla; Ruminantia; Pecora; Bovoidea; Bovidae; Bovinae; Bos. REFERENCE 1 (bases 1 to 805) AUTHORS Le Huerou,I. TITLE Direct Submission JOURNAL Submitted (28-AUG-1990) to the EMBL/GenBank/DDBJ databases. Le Huerou I., Centre National de la Recherche Scientifique, Centre de Biochimie et de Biologie Moleculaire, CBM3, 31, Chemin Joseph Aiguier, B.P. 71, 13402 Marseille Cedex 9, France REFERENCE 2 (bases 1 to 805) AUTHORS Le Huerou,I., Wicker,C., Guilloteau,P., Toullec,R. and Puigserver,A. TITLE Isolation and nucleotide sequence of cDNA clone for bovine pancreatic anionic trypsinogen. Structural identity within the trypsin family JOURNAL Eur. J. Biochem. 193 (3), 767-773 (1990) MEDLINE 91065383 COMMENT Data kindly reviewed (05-FEB-1991) by Huerou I. NCBI gi: 829 FEATURES Location/Qualifiers source 1..805 /organism="Bos taurus" /strain="Friesian Holstein" /dev_stage="adult" /tissue_type="pancreas" /clone_lib="pUC9" /clone="PB10" mRNA <1..805 CDS 9..752 /EC_number="3.4.21.4" /note="NCBI gi: 830" /codon_start=1 /product="trypsinogen anionic precursor" /translation="MHPLLILAFVGAAVAFPSDDDDKIVGGYTCAENSVPYQVSLNAG YHFCGGSLINDQWVVSAAHCYQYHIQVRLGEYNIDVLEGGEQFIDASKIIRHPKYSSW TLDNDILLIKLSTPAVINARVSTLLLPSACASAGTECLISGWGNTLSSGVNYPDLLQC LVAPLLSHADCEASYPGQITNNMICAGFLEGGKDSCQGDSGGPVACNGQLQGIVSWGY GCAQKGKPGVYTKVCNYVDWIQETIAANS" sig_peptide 9..53 misc_feature 54..77 /product="activation peptide" mat_peptide 78..749 /EC_number="3.4.21.4" /product="trypsin"