with: Katia Berdoldi and Tom Mullin

We have uncovered negative Poisson's ratio (auxetic) behavior in cellular solids that comprise a solid matrix with a square array of circular voids. The simplicity of the fabrication implies robust behavior, which is relevant over a range of scales. The behavior results from an elastic instability, which induces a pattern transformation and excellent quantitative agreement is found between experiment and numerical simulations.
Publications:
- K. Bertoldi, P.M. Reis, S. Willshaw and T. Mullin, "Negative Poisson’s Ratio Behavior Induced by an Elastic Instability", Adv. Mater. 21, 1 (2009) [html, pdf].
- "Materials Science: Squeezing Holes", Marc S. Levine, Editor's Choice: Highlights of the Recent Literature, Science 325, 1601 (2009). [html, pdf].
with: Benoit
Roman, Francis Corson, Arezki Boudadoud

We report a combined experimental and theoretical study of the compression of a solid foam coated
with a thin elastic film. Past a critical compression threshold, a pattern of localized folds emerges with a characteristic size that is imposed by an instability of the thin surface film. We perform optical surface measurements of the statistical properties of these localization zones and find that they are characterized by robust exponential tails in the strain distributions. Following a hybrid continuum and statistical approach, we develop a theory that accurately describes the nucleation and length scale of these structures and predicts the characteristic strains associated with the localized regions.
Publications:
Delamination of thin films from an elastic substrate
with: Dominic Vella, Benoit Roman, José Bico and Arezki Boudaoud
The
wrinkling and delamination of stiff thin films adhered to a polymer
substrate have important applications in `flexible electronics'.
The resulting periodic structures, when used for circuitry, have
remarkable mechanical properties since stretching or twisting of the
substrate is mostly accommodated through bending of the film,
which minimizes fatigue or fracture. To date, applications in
this context have used substrate patterning to create an anisotropic substrate-film adhesion energy, thereby producing a controlled array of delamination `blisters'. However, even in the absence of such patterning, blisters appear spontaneously, with a characteristic size. Here, we perform well-controlled experiments at macroscopic scales to study what sets the dimensions of these blisters in terms of the material properties and explain our results using a combination of scaling and analytical methods. As well as pointing to a novel method for determining the interfacial toughness our analysis suggests a number of design guidelines for the thin films used in flexible electronic applications. Crucially, we show that to avoid the possibility that delamination may cause fatigue damage, the thin film thickness must be greater than a critical value, which we determine. [Video here]
Publications:
- D. Vella, J. Bico, A. Boudadoud, B. Roman and P.M. Reis, "Delamination of thin elastic sheets adhered to an elastic substrate", Proc. Natl. Acad. Sci. U.S.A. 106, 10901 (2009) [html, pdf].
- MIT' Press release.
- "A curvy, stretchy future for electronics", John A. Rogers and Yonggang Huang, Commentry, Proc. Natl. Acad. Sci. U.S.A. 106, 10875 (2009) [html, pdf].
- "High Flex: failing stickers lead to research that could improve stretchable electronics" Technology Review, September/October 2009.
- Online press coverage of our article on delamination blisters [A22]: Nanowerk, Science Daily, EU-Cordis, Inside Engineer, ZDNet, Gizmag, Physorg, Frost & Sullivan
Tearing of thin adhesive sheets
with: Benoit
Roman, Enrique Cerda, and Eugenio Hamm

Thin adhesive films have become increasingly important in applications involving packaging, coating or for advertising. Once a film is adhered to a substrate, flaps can be detached by tearing and peeling, but they narrow and collapse in pointy shapes. Similar geometries are observed when peeling ultrathin films grown or deposited on a solid substrate, or skinning the natural protective cover of a ripe fruit. In this work, we have shown that the detached flaps have perfect triangular shapes with a well-defined vertex angle; this is a signature of the conversion of bending energy into surface energy of fracture and adhesion.In particular, this triangular shape of the tear encodes the mechanical parameters related to these three forms of energy and could form the basis of a quantitative assay for the mechanical characterization of thin adhesive films, nanofilms deposited on substrates or fruit skin.
Publications:
- E. Hamm, P.M. Reis, M. LeBlanc, B. Roman and E. Cerda, "Tearing as a test for mechanical characterization of thin adhesive films", Nature Materials, 96, 386 (2008), [html,pdf] Supplementary Material [html, pdf], Front Cover [html, pdf], [Video];
- "Material mechanics: An angle on sticky films", J. Groenewold, News and Views, Nature Materials 7 348 (2008). [html, pdf];
- "A Sticky Issue", D. Castelvecchi, Science News 173 12 (2008). [html];
- Audio coverage of our article on tearing of adhesive sheet [A16]:
Interview for NPR's (USA) "Morning Edition" (April 2, 2008) [Listen].
Interview of B. Roman for RTL's (France) "Le Journal de 7h" (April 29, 2008) [Listen].Interview of B. Roman for RSR's (Switzerland) "La Science de Pain" (May 26, 2008) [Listen].Scientific American 60-Second Science Podcast [Listen]. - International press coverage of our article on tearing of adhesive sheet [A16]:
MIT TechTalk (USA); MIT News Office Press Release (USA); El Mercurio (Chile); USACH Al Día (Chile); The Globe and Mail (Canada); Malaysia Sun (Malazya); Daily India (India); Ciência Hoje (Portugal); deFrente Algébrica (Portugal); KIJK (Holland); Publico (Spain); NyTeknik (Sweden); Pour la Science (France); Science et Avenir (France); Le figaro (France); La Croix (France); CNRS Press Release (France); Le Matin (Switzerland); GEO [pdf] (Germany); - Online press coverage of our article on tearing of adhesive sheet [A16]:
MIT Homepage, CNN, MSNBC, NanoWerk, Science Daily, Eurekalert, Physorg, Yahoo News, Live Science, Ars Technica, Inovations-Report, Science News Daily.
Mechanics of growth in plant tissue
with: Benoit
Roman, Mokthar Adda-Bedia, Arezki
Boudaoud and Francis Corson

Wether mechanical forces
have a role, or not, in the differentiation
and growth of plant tissue is still far from established. Two scenarios
in which this may be possible in the development of organs at the
meristem and of the venation network in leaves. It is, of course,
possible that such structures are purely geneticaly driven. However,
within a leaf, for example, it is known that differential growth between
the various layers of cells induces compressive stresses. Whether these
play any role in development is not known. Yves Couder et. al. have
recently put forward the idea that the striking similarities between
venation networks in leaves and the network of cracks in drying gels
suggests that a tensorial quantity, such as a stress, is at play.
Within the MechPlant European team, we are currently collaborating with
three plant biology groups (Bern, Jerusalem and Oxford) to develop
experimental settings in which to test these ideas.
Oscillatory Fracture in Thin Sheets
with: Benoit
Roman, Basile Audoly, Anil Kumar, Mark Shattuck and Simon de Villiers

Opening the plastic
packaging film of biscuit packs or CD cases has
never been easy, specially if one lacks a pen-knife in our pocket. One
way out is to use a key or a pen. If we use such a blunter object to
tear open the plastic, rather than observing a straight cut, the crack
follows a well defined and highly reproducible oscillatory path. We
have developed a well controlled experiment in which to study this
phenomena. Moreover, we have developed a geometrical 2D model that takes into
account bending and stretching of the thing plastic film. This simplemodel yields
results in excellent agreement with the experiments.
For more info and videos of the experiment please visit the following webpage.
Publications:
For more info and videos of the experiment please visit the following webpage.
Publications:
- P.M. Reis, A. Kumar, M.D. Shattuck and B. Roman, "Unizip Instabilities: straight to oscillatory transitions in the cutting of thin elastic sheets", Europhys. Lett. 82, 64002 (2008). [html,pdf]
- P.M. Reis, B. Roman and B. Audoly "Oscillating fracture paths in thin elastic sheets: when geometry rules the fracture path", Proceedings of the 16th European Conference on Fracture, Alexandroupolis, Greece, "Fracture of Nano and Engineering Materials and Structures", page 119 (Springer 2006). [pdf]
- B. Audoly, B. Roman and P.M. Reis, "Cracks in Brittle thin Sheets: When Geometry Rules the Fracture Path", Phys. Rev. Lett. 95, 025502 (2005). [html,pdf];
- B. Audoly, B. Roman and P.M. Reis, "Comment on The Cycloidal Wake of a cylinder Tearing Through a Thin Sheet", Phys, Rev. Lett. 94, 129601 (2005). [html,pdf];
- B. Roman, P.M. Reis, B. Audoly, S. de Villiers, V. Vignie and D. Vallet, "Oscillatory fracture paths in thin elastic sheets", C.R. de Mecanique 331, 881 (2003). [html,pdf]
- "Crumpling, buckling, and cracking: Elasticity of thin sheets", M. Marder, R. D. Deegan and E. Sharon, Physics Today 60 (2), 33 , February (2007). [html, pdf];
- "Cracked it", Research Highlights; Nature 436, 306 (2005). [pdf]
- "Envelope physics sheds light on ice sheets", Nature Science Update, 02 Dec (2003).
Uniformly Heated Granular Fluids: How far from equilibrium?
with:
Mark
Shattuck and Rohit Ingale

We
have developed an experimental system to study
Non-equilibrium steady states in a quasi-2D granular fluid in which
energy is injected uniformly across the cell. Using a number of classic
measures commonly used in statistical mechanics (Lindemann criterion,
radial distribution function, bond-order orientation parameter, shape
factor, intermediate scattering function, etc) we have shown that our
system assumes equilibrium-like structural configurations. Moreover, we
observe a fluid-to-crystal transition, as the filling fraction of the
granular layer is increased, exactly at the point at which it occurs
for equilibrium hard disks. Prior to crystallization, there is an
intermediate region in which caging of particles is dominant with a
relaxation timescale that follows a Vogel-Fulcher law, typical of
many glassy systems. Despite this strong equilibrium-like
behaviour,
non-equilibrium features are observed, as expected, in the dynamics of
the system as measured by deviations from Maxwellians of the
probability distribution functions of velocities.
Publications:
Publications:
- M. D. Shattuck, R. A. Ingale, and P.M. Reis, "Granular Thermodynamics", AIP Conf. Proc. 1145, 43 (2009) [html, pdf];
- P.M. Reis, R.A. Ingale and M.D. Shattuck, "Forcing independent velocity distributions in an experimental granular fluid", Phys. Rev. E 74, 051311 (2007). [html,pdf]
- P.M. Reis, R.A. Ingale and M.D. Shattuck, "Caging dynamics in a granular fluid", Phys. Rev. Lett. 98, 188301 (2007). [html,pdf];
- P.M. Reis, R.A. Ingale and M.D. Shattuck, "Crystallization of a quasi-two-dimensional granular fluid", Phys. Rev. Lett. 96, 258001 (2006). [html,pdf];
Segregation in granular binary mixtures
with:
Tom
Mullin, George Ehrhardt and Andrew Stephenson

An
interesting and counter-intuitive issue in the collective behavior
granular materials is the segregation of binary assemblies, where an
initially uniform mixture of particles can spontaneously de-mix under
flow. During my Ph.D. I developed an experimental physical model system
in which to study segregation of binary mixtures of particles. I
constructed an approximately two-dimensional precision apparatus
consisting of a monolayer driven by the frictional forces with the
surface of an oscillatory tray. Systematically starting from
homogeneously mixed initial conditions, I uncovered the existence and
self-organisation of three phases of segregation, as a function of the
total filling fraction of the layer. The foremost result was the
discovery a critical phenomena in granular segregation. This implies
the existence of a transition point in below which the layer remains
mixed and above which segregation occurs. This behaviour had
characteristics of continuous phase transitions, usually observed in
well understood equilibrium statistical mechanical systems.
Publications:
Publications:
- P.M. Reis, T. Sykes and T. Mullin, "Phases of granular segregation in a binary mixture", Phys. Rev. E 74, 051306 (2006). [html,pdf];
- G. Ehrhardt, A. Stephenson and P.M. Reis, "Segregation Mechanisms in a Numerical Model of a Binary Granular Mixture", Phys. Rev. E 71, 041301 2005 . [html,pdf]
- P.M. Reis, G. Ehrhardt, A. Stephenson and T. Mullin, "Gases, Liquids and Crystals in Granular Segregation", Europhys. Lett. 66, 357 (2004). [html,pdf]
- P.M. Reis and T. Mullin, "Granular Segregation as a Critical Phenomenon", Phys. Rev. Lett. 89, 244301 (2002). [html,pdf]
- "Granular Games", Nature Materials, 2 (1), 6 (2003).
- "A Poor Mix", Research Highlights, Nature Physics Portal, 25 Nov (2002).
Research